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The esterification reactions were carried out under a slow stream of deoxygenated nitrogen.
The samples were then cooled to room temperature, and the excess reagent was removed under a slow stream of dry nitrogen.
A mixture of N,N-diethylaniline 1 (27.0 g, 0.2 mol) and cyanuric chloride 2 (18.4 g, 0.1 mol) was heated at 70°C for 8 h under a slow stream of dry nitrogen.
The extract was gravity-drained into a round bottom flask, and rotary-evaporated at 47-52°C 47-52°C5 mL, toen dried under a slow stream of nitrogen at 40°ca
The eluate was evaporated to a small volume under a slow stream on nitrogen using 200 μL isooctane as a keep solvent.
Samples were then centrifuged and the extract was concentrated under a slow stream of nitrogen at 50° C to 2 mL.
Similar(52)
With blender running, add grape seed oil in a slow stream until fully incorporated.
Incorporate the ingredients into the egg and sugar mixture in a slow stream.
Stir in olive oil in a slow stream.
Add melted butter in a slow stream and fold into the batter with a rubber spatula.
Pee with a forceful stream for a smaller panty stain, or with a slow stream for a more pleasurable time.
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