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We have also used an ultra micro balance to determine the mass and mean single-layer surface coverage of each multilayer.
The coatings were characterized with respect to microhardness using an ultra micro hardness tester Fisher HV100P and with respect to the abrasive wear resistance using a mechanical simulator for hip prosthesis developed in our laboratory.
While thin blends were totally amorphous and possessed ultra micro heterogeneity, thicker-film blends possessed much greater scales of heterogeneity and developed solvent-induced PC crystallinity, which could suppress the Tg of the PC phase.
The reaction was stopped by mixing with 5 µL formic acid, and the protein was freed from the buffer salts using an Ultra Micro Spin C18 column (Nest Group, Southboro, MA) according to the manufacturer's instructions and dried in a Speed Vac.
Macroscale pH measurements with the In-Lab Ultra Micro pH meter showed a pH change of −1.24 units for the complete full reaction.
Separate calibration experiments using an In-Lab Ultra Micro pH Probe from Mettler Toledo were completed to quantify the pH response from a given NaOH or HCl addition event (see Supporting Information Figure S-1).
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He still remembered the title of my project my junior year: "Ultra Micro-Miniature Thumb-Sized Digital Calculator With a Novel Nematic Liquid Crystal for the Display".
Mechanical properties of the nanocrystalline surface layer were investigated using dynamic ultra micro-hardness tester.
The H2 generated during corrosion of magnesium is oxidized at the probe(i.e. a Pt ultra micro-electrode);with the magnitude of the current generated due to oxidation being indicative of the intensity of H2 evolution at a local scale on the magnesium surface.
Colorimetric quantification was determined by an EL808 Ultra Micro-plate Reader (Bio-Tek Instruments, Inc) after the addition of formazan dissolved in 25% N, N-dimethylformamide and 10% SDS under light-proof conditions overnight. 1 × 105 cells (U2OS or RD2) were seeded on sterile coverslips in a 6-well plate overnight.
The mechanical properties of BCN films were evaluated using an ultra-micro-hardness tester.
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