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Figure AF3 GC-FID spectra of biotransformation detection: retention time at 8.82 min was identified as 3(Z -nonenal.

HDI monomer eluting at 9.35 min was identified in all the pyrograms produced for water-dispersible polyisocyanate resins.

This peak eluting at 3.01 min was identified as 1-hexene based on its molecular ion fragmentation pattern characterized by m/e of 84.

An optimum treatment, with electric field 600 V/cm and treatment time 3 min, was identified to accelerate wine aging, which made the harsh and pungent raw wine become harmonious and dainty.

The optimal formulation which showed the fastest release rate (more than 80% in first 30 min) was identified (compression force of 8 kN, 20% of Labrafil® 2130CS, 10% of Cremophor® RH40, 30% of carbamazepine, 5% of crospovidone NP and Neusilin® UFL2 used as the carrier).

The product with parent ion m/z 249 at 6.08 min was identified as ring dihydroxylated molecule with one methyl group missing, while the one with m/z 277 at 5.31 min as ring dihydroxylated product with one methyl group oxidized to -CHO.

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Interestingly, the IPDI monomer, eluting at 10.86 min is identified as well.

In the GC spectra, peaks at 8.82 min were identified as 3(Z -nonenal (Additional file 1: Figure AF3).

Many linear alkanes and four trimethylsilylated metabolites, which had retention times of 10.68, 13.19, 15.33 and 18.07 min were identified as 1, 2-benzenediol, benzoic acid, 1,2-benzenedicarboxylic acid and phthalic acid, respectively (Fig. 7).

Peaks observed at tR 16.7 – 19.7 min were identified as ellagitannins.

Respondents who completed the survey in less than 15 min were identified as speeders and excluded from the analyses.

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