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The design of each monochromator is quite similar with the exception of the silicon crystal reflections that are used and the surface asymmetry angles that are chosen.
Equatorial scattering maxima in the SAXS patterns for samples annealed at 75 °C were observed before the appearance of crystal reflections.
In this way it became possible to measure the development of crystal reflections as a function of the distance from the spinneret.
For take-up speeds of 3600 m/min and higher, the crystal reflections appeared at a distance of 40 cm from the spinneret, just after the necking region.
At low draw ratios or low PVC contents, all the observable (hk0) crystal reflections orient towards the meridional direction in WAXD patterns, indicating the presence of ring-fibre orientation.
WAXD spectra of the polymers are shown in Figure 5(a) and corresponding d-spacing and Miller indices of the crystal reflections are listed in Table 2.
Similar(54)
From SWAXS measurements, the appearance of the SAXS peak appears to occur prior to WAXD crystal reflection peaks, suggesting that density fluctuations are probably present before melt crystallization.
The crystal orientation was obtained in terms of the Herman's orientation function f2 from the azimuthal scan of the (200) crystal reflection.
SHELXT automates routine small-molecule structure determination starting from single-crystal reflection data, the Laue group and a reasonable guess as to which elements might be present.
The new computer program SHELXT employs a novel dual-space algorithm to solve the phase problem for single-crystal reflection data expanded to the space group P1.
At the highest total dose-rate, the crystal lattice reflections were all absent.
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