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In general, the polymerization proceeded very fast and most of the monomers are consumed in less than 1 min. Attempts to withdraw samples at various intervals for kinetics analysis were not successful.
An additional complication in the context of banking samples from cancer patients is determining who has the authority to withdraw samples when there is no legal will or declaration of a proxy.
Core needle biopsy (CNB): This procedure uses a wide-diameter needle to withdraw samples of tissue up to.5 inches (1.27 cm) long.
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Encapsulation efficiency of withdrawn samples was determined.
A quantitative GC FID analysis of the withdrawn samples was performed.
The withdrawn samples were analyzed for drug content by spectrophotometer at 476 nm (Fig. 4).
Radial concentration profiles were measured at various downstream distances by withdrawing samples from the flow and measuring their electrical conductivity.
OD, redox potential (Eh) and pH of withdrawn samples was measured instantly using EUTECH Instruments (pH and Eh Tutor).
The withdrawn samples were used for OD measurement at 237 nm by a UV-visible spectrophotometer (Shimadzu, model UV-2601).
The experiments were conducted at atmospheric pressure by withdrawing samples from the flame using a quartz microprobe coupled to an online gas chromatograph (GC).
All withdrawn samples from the reaction media during the process showed no antibacterial activity, which indicates safety of the treated effluent for disposal into the environment.
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