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A wider calibration range can be achieved by applying a quadratic calibration equation (data not shown and not further pursued for the purpose of this study).
For the analyses of medicated feed there was a need for a wider calibration curve (10 100 mg/kg), which was also tested to be linear over the range.
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The BLM v.2.2.3 was used since it has a wide calibration range and uses a conversion factor to transform acute to chronic data.
The developed PEC method possessed a wide calibration range from 1.0 pg mL−1 to 50 ng mL−1 and a low detection limit of 0.63 pg mL−1.
It also allowed wide calibration curves to be established that were adapted to this quantification in MDs during migration tests, irrespective of the amount present, and while maintaining good precision and accuracy.
This gives several advantages over the previous manufacturing techniques and offers a general and flexible scheme for the fabrication of biosensors presenting high sensitivities, wide calibration ranges and less affected by electrochemical interferences.
Under optimal working conditions, MeJA showed a wide calibration range of 5.0 × 10−7 to 8.0 × 10−5 M with a low detection limit of 2.0 × 10−7 M by using the derivative differential pulse voltammetry.
Using clenbuterol as model analyte, the ECL intensity was determined by the concentration of competitive immunoassay of clenbuterol with a wide calibration in the range of 0.05 ng mL−1 to 1000 ng mL−1, and a low detection limit was 0.02 ng mL−1.
Since efficient electron transfer between glucose oxidase and the electrode was achieved, the biosensor showed high sensitivity (5762.8 nA nM−1 cm−2), low detection limit (S/N = 3) (3 × 10−12 M), fast response time (0.045 s), wide calibration range (from 1 × 10−11 M to 1 × 10−8 M) and good long-term stability (26 weeks).
The 95% confidence intervals of older divergence events are large compared to most of the more recent events, as we allowed for a wide calibration range for the root node.
Full calibration curves of the 19 compounds were obtained with relatively wide concentration ranges, and the correlation coefficients of all the calibration curves were greater than 0.9990.
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