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Cluster 1 crystallized after eight weeks, yield 200 mg (43 %).
Cluster 8 crystallized after 12 weeks, yield 100 mg (26%%).
Cluster 5 crystallized after three weeks, yield 100 mg (20%%).
Reddish-brown crystals were obtained after two weeks, yield 0.120 g (41%% rel. Ti).
Crystals of 4 were obtained after three weeks, yield 500 mg (48%%).
The ALLY-3 trial using the same regimen without RBV for 12 weeks yield SVRof90%0% in treatment-naïve and 86% in treatment-experienced patients.
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