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Fraction D was separated over RP-18 (MeOH/H20 100–100 %) into fractions D1 D4.
Fraction B (86.4 g) was separated over a MCI-gel column (MeOH-H2O from 8 2 to 10 0) to obtain five fractions (Fr. B1 B5).
B3 (27 g) was separated over a MCI-gel column (MeOH-H2O from 85:15 to 100 0) to obtain six fractions (Fr. B3a B3f).
Fraction B (223 g) was separated over a MCI gel column (MeOH-H2O from 70 30 to 100 0) to obtain eight fractions (Fr. B1 B8).
Subfraction B (54 g) was separated over an MCI-gel column (MeOH H2O from 3 2 to 10 0) to obtain five fractions (Fr. B1 B5).
C (30.0 g) was separated over an MCI gel column (MeOH/H2O from 4 6 to 10 0) to obtain four fractions (Fr. C1 C4).
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