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The reaction solution was cooled to room temperature.
After that, the autoclave was cooled to room temperature naturally.
The resulting sol was cooled to room temperature.
After reduction, the reactor was cooled to 320 °C.
After completion, the reaction was cooled to rt, diluted with water and extracted with EtOAc (x3).
The sample stage was cooled to 20 °C by a circulating thermostat (Huber CC-K6).
Thereupon the mixture was cooled to room temperature and then added portionwise to saturated aqueous NaHCO3.
Then, the reaction mixture was cooled to room temperature and precipitated with 50 ml of water.
Then, the flask was cooled to room temperature and water was added.
The reaction was cooled to rt and diluted with water and extracted with EtOAc (x3).
The solution was cooled to −78 °C (dry ice/acetone bath), monitored by a thermocouple.
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