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The etching process was characterized with a statistical experimental design.
The capacitance was characterized with a Wayne Kerr 6500B impedance analyzer.
The morphology and microstructure of the samples was characterized with a transmission electron microscope (TEM, Tecnai G2 F20 S-Twin).
The powder morphology of the samples was characterized with a FEI Quanta 200 environmental scanning electron microscope.
Before going for TEM observation, the memory device was characterized with a program/erase of 4,000 cycles.
The coating adhesion was characterized with a conventional scratch tester (CSEM Revetest).
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Surface morphology was characterized with an environmental scanning electron microscope (SEM, model Hitachi TM1000).
The surface morphology of the thin films was characterized with an atomic force microscope (Park Scientific Instruments, CA, USA) under ambient conditions.
The topography of these nanostructures was characterized with an Asylum Research MFP-3D atomic force microscope (AFM) (Asylum Research, an Oxford Instruments Company, Santa Barbara, CA, USA).
The thermal protection performance of the material system was characterized with an oxy-acetylene flame ablation test.
For use in the finite element model, emissivity was characterized through infrared image analysis, and thermal conductivity was characterized with an inverse method.
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