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Kilbride, P. et al. Spatial considerations during cryopreservation of a large volume sample.
In addition, an on-line concentration method of large volume sample stacking was designed.
Due to the small test cell volume, sample in situ experiments are not foreseen.
The studied variables were drop volume, sample volume, agitation speed, ionic strength, extraction time and ethanol quantity.
A large volume sample stacking (LVSS sweeping CE is developed for concentrating and analyzing the 10 abused drugs.
Vial volume, sample volume/vial volume ratio, pH, adsorption time and temperature have been optimised by means of two experimental designs.
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With careful design of the loading sequence and volume (sample--precipitating reagent--sample), simultaneous detection of sucrose and phosphate was accomplished with the single PEDD detector.
The overpotential predicted with the largest volume size sample is slightly larger than those of smaller volume samples.
The urine volume corresponded to the volume sampled during the last hour of resuscitation.
The immobilized DMC can be used on large volume samples and at low metallic pollutant concentrations.
Moreover it offers the precise control of nano/picoliter volume samples.
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