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Figures 4 and 5 are representative TGA and DTG curves of treated and virgin samples.
θ 2θ XRD diffractograms of the virgin samples C0 showed only peaks associated to <100> ZnO (Fig. 2a).
Fusion zone of all the welded samples have reported lower Young׳s modulus and higher yield strength compared to virgin samples.
CaCO3 crystalline diffraction peaks are shown in the virgin samples at 27.32, 33.23, 36.29 and 43.07 (Heredia et al. 2007; Mikkelsen et al. 1997).
However, the yield of the Zn atoms decreased beyond channel 427 compared to the random level in the case of virgin samples C0.
After self-healing, flexural stiffness was also retained significantly compared with that from virgin samples, even though the level of retaining decreases with the increase of precracking time.
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This was not seen in the virgin sample.
Annealed samples show wide terraces running parallel to the original steps in the virgin sample.
They occur in the virgin sample as minute grains and are finely disseminated throughout.
The response of welded samples in the elastic and plastic region is compared with the virgin sample.
The size of the grains in the SEM images of MW samples was smaller than in the virgin sample.
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