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Drying runs are done on 45.5 kg and 227.3 kg of wet coconut meat in the continuous vent mode and the intermittent vent mode of the dryer.
The amino acid derivatives were injected into a J&W DB-23 column (60 m × 0.32 mm i.d., 0.52 μm film thickness, Agilent Technologies) using the PTV injector in solvent vent mode.
This also works for your car: keep the windows closed and the air conditioning on "recycle" rather than vent mode.
The PTV was operated in the solvent vent mode in order to evaporate the LC effluent.
We cryofocused each 25-μl sample in the Gerstel CIS-4 held at –10 °C and injected the sample in solvent vent mode with an injector temperature of –10 °C.
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For the intermittent venting mode the time for drying was 120 hours and the energy was 581.4 MJ.
It was found that for the continuous venting mode the time taken to dry 45.5 kg of wet coconut from 50% to 7% moisture content dry basis (me db) is 168 hours and the energy used was 683.7 MJ.
For PTV injection in solvent-vent mode 20 μL was injected at 5 μL s−1.
On injection of 20 μL standard in ethyl acetate toluene, 8 2, in the solvent-vent mode, no peak distortion was observed, indicating that less then 2 μL toluene remained in the injector after the solvent-vent step.
For the GC/MS analysis, 10 μl of sample extract was injected into the PTV injector in split-vent mode at an initial temperature of 55°C for 0.5 min at a vent flow of 100 ml/min; the temperature was then ramped up at 600°C/min to 400°C with a 15 min static time.
On the condition of optimum air vent management mode, surface and average temperature of heat storage wall computer simulations were run with CFD to analyze the heat storage and release performance of trombe wall.
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Justyna Jupowicz-Kozak
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