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The variable microscope aperture was adjusted from approximately 60 μm × 60 μm to 100 μm × 100 μm).
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For the present study, a Tescan variable pressure scanning electron microscope, a JEOL 6400 scanning electron microscope, and a Hitachi S-3400 N scanning electron microscope were used with the same sherd.
variable pressure-scanning electron microscope.
The predicted samples were characterized by X-ray diffractometer (XRD), scanning electron microscope (SEM), variable pressure scanning electron microscope (VPSEM) and Energy-dispersive X-ray (EDX).
SEM images were recorded on a Zeiss 1450EP (Carl Zeiss AG, Oberkochen, Germany) variable pressure scanning electron microscope.
On return to the laboratory, the stacked foils are separated for examination in a variable pressure scanning electron microscope, without need for surface coating.
The images and maps produced by the Tescan variable pressure scanning electron microscope did not always show well-defined iron-based pigmented areas on the sherd.
SEM EDX analysis was carried out using a Carl Zeiss EVO® MA10 variable pressure scanning electron microscope (SEM) coupled to an Oxford Instruments X-Max 80 mm2 energy dispersive X-ray spectrometer, using INCA 350 software.
Small samples of metal-wrapped threads were taken from the textiles and the metal wrappings examined using an Oxford Instruments INCA Energy 300 Microanalysis system energy dispersive X-ray spectrometer with a LEO 1455 variable pressure scanning electron microscope, operated at an accelerating voltage of 20.0 kV.
A Tescan VEGA 3 XMU variable pressure scanning electron microscope (VP-SEM) was used for this study equipped with two Everhart Thornley type secondary detectors: a low vacuum secondary Tescan detector (LVSTD) and another Everhart Thornley secondary detector for use with vacuum settings near 2.3e−2 Pa.
The paper considers some major problems of adapting the multi-detector method for three-dimensional (3D) imaging of wet bio-medical samples in Variable Pressure/Environmental Scanning Electron Microscope (VP/ESEM).
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