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The vacuum stage led to the separation of cross-linked elastomer (top) and ceramic (bottom) phases.
In addition, the aerosol is sampled into the first vacuum stage of a mass spectrometer through a capillary, which can be heated to aid further solvent evaporation from the charged droplets.
For deposition at 1 × 10-2 Pa, the high vacuum stage, a turbo-molecular pump, is engaged for only 5 min, after the roughing pressure has been reached; the base pressure reaches 5 × 10 -3 Pa, and the working pressure is 1 × 10-2 Pa.
In the heated capillary ESI-MS interface, desolvation occurs dominantly in the higher pressure region inside the heated capillary as the charged droplets are transmitted from ambient pressures to the first vacuum stage of the instrument.
In the SPIN source, the ESI emitter is moved from the atmospheric pressure environment, as used in any conventional ESI source design, into the first vacuum stage of the mass spectrometer with its operating pressures typically of 15 30 Torr.
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As they dithered, Mr Carmona stepped opportunistically into the power vacuum, staging "a coup within a popular uprising".
In parallel to integration of the PDT ion optics, a test bench for a vertical vacuum wafer stage has been realized by Leica.
The effect of a short vacuum heating stage prior to oxidation on the kinetics, surface scale composition and roughness has been investigated.
Scaling-up is based upon successful studying, evaluation and optimization of all operating parameters affecting process chemical reaction kinetics, product recovery and purification, and finally the vacuum crystallization stage.
Dynamic image analysis confirmed that minimum attrition of COA was achieved when (a) the majority of the methanol was removed during pressure filtration at 0.5 bar N2 and (b) intermittent agitation was applied during the vacuum drying stage.
LT-FDM is performed using a high vacuum cold stage.
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