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The thermal degradation was studied in an inert (N2) atmosphere from ambient temperature to a temperature of 600 °C using a heating rate of 10, 20, 30, 50, 100 °C min−1.
Thermal properties of the materials were investigated on a PerkinElmer Simultaneous Thermal Analyzer (STA 6000) using a heating rate of 10 °C.min−1 under air flow.
Thermogravimetry of the sample was made in the air on a Model Thermo Plus TG8120 equipment (Rigaku, Tokyo), using a heating rate of 10 °C/min.
Thermogravimetric (TG) results were obtained by a thermal analysis system (Q600, TA, USA) using a heating rate of 10 °C min− 1 in air.
Calcination of the dried nanosheets was performed in flowing oxygen gas (200 mL/min), using a heating rate of 5 °C/min at the ramp stage and a holding time of 4 h.
Thermogravimetric analysis (TGA) for the samples was performed on a Perkin Elmer diamond thermal analyzer from room temperature to 600 °C, using a heating rate of 10 °C/min with N2 as the sample purge gas.
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Qin et al. used a heating rate of 10°C/min, which is higher than the one used here.
Two types of Macro-TG apparatuses were used; the first was non-isothermal and was used at a heating rate of 20 °C/min, and the second was isothermal used at two temperatures, 400 °C and 600 °C.
Isothermal vacuum annealing treatments for 1 h at temperatures up to 1000 °C were performed at a base pressure of ⩽5 × 10−4 Pa using a heating and cooling rate of 20 and 50 K min−1, respectively.
During the heating process, Ar flow was firstly used with a heating rate of 5 °C min−1.
The reaction order of lubricant depletion is evaluated during the rapid heating using a constant heating rate and various coverages.
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