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Thermogravimetric analysis (TGA) was conducted with a Cahn TG131 TGA system (Cerritos, CA, USA) at a heating rate of 20°C/min under nitrogen atmosphere from room temperature to 850°C.
The thermal behavior of the precursor complex was studied using a Netzsch STA 409 PC/PG thermal analyzer (Netzsch, Burlington, MA, USA) at a heating rate of 5°C min-1 in air.
Weight loss temperatures of the products were measured with a TA thermogravimetric analyzer (TGA 2950, TA Instruments, New Castle, DE, USA) at a heating rate of 20°C/min in N2 atmosphere.
Thermogravimetric analysis (TGA) was performed using a Perkin-Elmer, Diamond TG/DTA (Perkin Elmer, Waltham, MA, USA) at a heating rate of 10 °C/min under a nitrogen atmosphere.
The interaction between inorganic core and organic shell was examined by FTIR operated on an IR-200 (Thermo Electron Co., U.S .. Thermal-gravimetry analysis (TGA) was conducted on a Pyrisl analyzer (PE Co., USA) at a heating rate of 10 °C/min under nitrogen protection.
DSC analysis was carried out by using DSCQ20 (TA Instruments, USA) at a heating rate of 10°C/min in the range of 40 220°C.
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The thermal degradation analysis of SEBS, grafted SEBS, and their nanocomposites was performed withTGA Q50 of TA Instruments- Waters LLC, USA operated at a heating rate of 20 °C/min in N2atmosphere at a flow rate of 60 mL/min in the temperature range of 25 700 °C.
Thermograms for P. pinnata seed hull fibres and isolated cellulose fibres were determined using a thermogravimetric analyser (TGA Q50, TA instruments, USA) at a 10 °C/min heating rate in nitrogen atmosphere.
The thermal decomposition processes of the samples were characterized by DSC using Dupont (Wilmington, DE, USA) 2000 instrument at a heating rate of 10°C/min.
NCF thermal stability in air was studied by thermogravimetric analysis (TGA, SETARAM Setsys Evolution, Hillsborough, NJ, USA; samples were analyzed in Pt pans at a heating rate of 10°C/min up to 850°C in an atmosphere of air flowing at 100 mL/min).
Thermogravimetric analysis (TGA) was performed under a nitrogen atmosphere at a heating rate of 10°C/min (Q50, TA Instruments, New Castle, DE, USA).
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