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The solid residue mainly precipitated asphaltenes was rinsed with 40 mL of the liquid precipitant until a clear solvent was obtained.
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A clear solvent solution serves as the reference blank.
Methylene chloride was evaporated under a nitrogen stream until a clear solution was obtained.
Methylene chloride was evaporated under a nitrogen stream until a clear solution obtained.
The solution was then refluxed for 1 h until a clear solution was obtained.
The mixture was stirred at room temperature until a clear solution is formed.
Then, the two solutions were mixed and stirred at room temperature until a clear solution formed.
The suspension was heated until a clear solution was obtained.
HCl was added dropwise until a clear solution was obtained.
The mixture was heated until a clear solution was obtained.
This process was repeated until a clear color solvent was observed.
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