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The contents were further heated at 55 °C overnight under total reflux and stirring.
In addition, distillation tests with standard test mixtures under total reflux conditions were conducted.
The extraction was carried out for 1 h at 180 °C under total reflux with the help of a reflux condenser (Christy et al. 1992).
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Various solvent blends were employed for the coal extraction under the total reflux condition.
Experiments were carried out at total reflux condition.
The present work proposes a novel cyclic total reflux (CTR) operation of batch distillation with two reflux drums working alternatively.
This method can be used to find the minimum reflux ratio, minimum number of stages at total reflux, and number of stages at given reflux ratio, as well as the reflux ratio with given number of stages.
The computational comparison of the novel policy with the regular constant reflux and non-cyclic total reflux (NCTR) operations is also presented.
Surprisingly, the continuous operation performance appeared slightly better than in case of the total reflux operation.
At the operating conditions studied, the separation was equivalent to 0.9 2.7 equilibrium stages, assuming total reflux.
In this work, we incorporate multistage reactive rectification and reactive stripping models with total reflux and total reboil, respectively.
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