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Exact(1)
Fractions eluting between 8.5-9.2 8.5-9.2e collected, concentrated to 10 minunder slight vacuum (200 mbar) and further evaporated to dryness under high vacuum at a temperature betwere -60°collected.
Similar(59)
When the rarefication wave reaches the other (open) end of the tube, air rushes in to fill the slight vacuum.
Slight vacuum was applied to facilitate substrate infiltration.
The reservoir was removed and the IAC drained, applying slight vacuum to drain fully.
The mixture was dried to a thin film under vacuum.
Vac.: Under a vacuum condition.
HF excess and scavenger were eliminated under high vacuum.
All washes were performed under mild vacuum.
Trace solvents were removed under high vacuum.
The volatiles were removed under fine vacuum.
The excess alcohol was evaporated under high vacuum.
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