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Then, the tube was cooled down to room temperature under a continuous argon flow.
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(a) FE-SEM image of sample S1 obtained under continuous argon gas flow and (b) a magnified image.
The surface, now bearing acid terminations, was introduced into a Schlenk tube containing a solution mixture of 5 mM EDC and 5 mM NHS and allowed to react under continuous argon bubbling for 90 min in a water bath at 15°C.
The reaction mixture was immersed in an oil bath maintained at 150°C and kept under a continuous flow of argon.
Thin films with a thickness of 20 nm have been deposited on glass substrates at room temperature under a continuous flow (50 sccm) of argon.
All reactions were performed under a dry argon atmosphere.
All reactions were carried out under a protective argon atmosphere.
The reaction was carried out under a protective argon atmosphere using standard Schlenk techniques.
All reactions were carried out under a protective argon atmosphere by using standard Schlenk techniques.
The mixture was filtered through a sintered glass filter of medium porosity (G02) under a flowing argon blanket.
APS-mica was washed with water, dried under a stream of argon and then cured overnight and stored under argon at reduced pressure.
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