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Exact(10)
The sample was stirred for homogenization.
For analysis, the SPME fiber (divinylbenzene/Carboxen on polydimethylsiloxane by Supelco) (Bellefonte, PA) was exposed to the vial headspace while the sample was stirred for 45 minutes.
For removal of apatite, 0.8 M HCl was added and the sample was stirred at 10°C for 30 minutes.
To avoid singlet-triplet annihilation, the sample was stirred with a magnet bar.
During extraction the sample was stirred at 500 rpm and maintained at 80°C.
The sample was stirred for 3 h and then filtered through a syringe filter.
Similar(50)
All of the samples were stirred for 24 h and 1,200 rpm using a magnetic stirring plate.
The samples were stirred in Teflon-lined amber glass bottles overnight with a glass-coated magnetic stirring bar.
The samples were stirred for 2 h at 800 RPM.
The samples were stirred continuously throughout the experiment.
On the other hand, lower dehydrochlorination yields were measured when the samples were stirred.
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