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Nevertheless, the two-day delay allowed Braun's lawyers to successfully raise doubts about the manner in which the sample was handled.
The sample was handled twice, with and without the step of phosphite oxidation to phosphate, and the formed orthophosphate was quantified after interaction with the vanadate-molybdate reagent.
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Workers were unlikely to have been exposed, however, because the samples were handled under enhanced biosafety-level 3 conditions, which includes many safety measures such as workers wearing protective suits and respirators.
Every day, the samples were handled independently and the standard curves were freshly made.
The samples were handled as described for the experiment in orbit.
Because all of the samples were handled in the same manner and for the same length of time, dessication of samples should not be expected to affect results.
The samples were handled anonymously and all donors gave consent to the blood being used for this purpose and the sampling was approved by the local ethics committee.
The present results suggest that valid measurement can be done within several days after collection if the samples are handled appropriately.
All the samples were handled in a coded fashion, according to National ethical guidelines ('Code for Proper Secondary Use of Human Tissue', Dutch Federation of Medical Scientific Societies).
In a 2-1 vothe the panel that heard Braun's appeal agreed that valid questions had been raised about the manner in which the test sample was handled.
Braun tested positive for elevated testosterone in October 2011, but successfully overturned a 50-game penalty when an arbitrator ruled the outfielder's urine sample was handled improperly.
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CEO of Professional Science Editing for Scientists @ prosciediting.com