Exact(3)
The increase of scanning speed plays an important role to avoid motion artifacts.
The layer-band-like zone, which consists of coarse basket-weave microstructure with short-lamellar α phase and β phase, decreases with the increase of scanning speed.
With the increase of scanning rate, the potential separation between the cathodic peak and anodic peak of TiO2 nanorod array become more and more larger, suggesting the increased polarization.
Similar(57)
The specific capacitances of all samples decrease as the increase of scan rates.
As shown in Fig. 5a e, with the increase of scan rates, the redox peaks shift to higher and lower potentials, respectively.
It indicates that the irreversible degree and the quasi-reversible reaction are increased with the increase of scan rate [36, 41].
These specific capacitances decrease with the increase of scan rate, probably due to an increase of ion diffusion-related resistance [39].
In addition, the observed peak potential shift to a more negative values on the increase of scan rate confirmed the irreversible nature of the studied cathodic reduction process.
With the increase of scan rate, the cathodic peak current densities and potentials gradually and regularly shift negatively, and the corresponding anodic peak current densities and potentials shift positively with increasing scan rates.
The corresponding plot in the Fig. 3a shows that the oxidation and reduction peak currents of released p-NP increase linearly with the increase of scan rate from 5 to 30 mV/s.
It was noted that the peak position shifted slightly with the increase of scan rate, implying a good capacitive behavior and a high-rate capability of the electrode material.
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