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Compared with the traditional hydrocyclone, the LLCR consists of two kinds of inlets, one for the light phase and one for the heavy phase.
Compared with the traditional hydrocyclone, the novel cyclone reactor consists of two inlets, one for the light phase and one for the heavy phase.
The starting point was a previous study on the same subject, which considered that no solute is lost in the vapor phase and a fixed fraction of 2% of the CO2 is lost within the heavy phase.
The light phase is injected into the reactor through two symmetric tangential slots in the inlet, while the heavy phase inlet is an axial entry with a guide vane.
The column is not a good design as the number of trays between the feed inlet and the azeotropic side stream (6 trays) is not sufficient to prevent some acetic acid of the feed stream from reaching the side stream, so that the "raw furfural" (the heavy phase of the decanter) must be submitted to a massive neutralization.
Measurement of the heavy phase layer thickness, using image analysis based on the Young Laplace theory for interface shape, and measurement of volume flow rate of each phase and pressure and temperature in the spiral channel allows rigorous comparisons with an existing 'wide-channel' model relating flow rates and layer thicknesses to phase properties, geometry and rotation rate.
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At the end of the reaction, a biphasic system was obtained in which the upper methanolic phase, which contained most of the starting catalyst, was separated from the heaviest phase, mainly composed of fatty acid methyl esters.
It was built during the heaviest phase of fighting for an immense sum - $740 million dollars - with specs set by pessimists who assumed mortars would be fired at it for years.
The measured thickness of the heavy-phase layer is predicted well by the wide-channel model at high rotation and phase flow rates, where the deviation from a uniform layer thickness due to menisci at the channel end walls and interface tilt from gravity are small.
As expected the dsDNA concentration of the USD heavy phase stream was significantly lower compared to the pilot scale process stream.
In this study, the yield of the product (heavy phase) from MD was 53.1 ± 0.4%.
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