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Spiking of extracts is justified when the extraction efficiency is very high (above 90%) for all relevant toxins.
The first 10 samples were extracted three times to determine the extraction efficiency.
To determine the extraction efficiency, two naturally contaminated shellfish samples were extracted with methanol (4 times) and acetone (once).
Cs-137 was measured to confirm the extraction efficiency.
Then, we took the average value on the extraction efficiency.
After this time, the extraction efficiency was not increased significantly.
Parameters affecting the extraction efficiency were investigated in detail.
The extraction efficiency (i.e. recovery) of triglycerides reached 96.77%.
The extraction efficiency in terms of percent recovery from various samples was investigated.
The addition of formic acid improved the extraction efficiency of salvianolic acid B and Danshensu.
The extraction efficiency was monitored relative to the total radioactivity in aliquots.
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