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A partial least squares analysis using these values gave correlation equations for the experimental yields.
The experimental yields of carbonaceous materials relative to the starting materials are about 8.0 14.4% (w/w).
Under these conditions, the experimental yields of EnPPs reached 3.61%, which were in good agreement with the validated values (3.57 ± 0.51%).
It also seems that the experimental yields decrease for combinations of substrates with lower theoretical yields.
However, the experimental yields tend to be lower than theoretical ones.
This is because the experimental yields measured at 155°C and 170°C were compromised by the automated heating time of the Dionex™ ASE™ 350.
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Under these conditions, the experimental yield was 6.69%.
We notice that the largest pathway is H+ formation, which is in agreement with the experimental yield as the H+ ion peak is the strongest.
Under optimized conditions, the experimental yield 7.97 ± 0.27% agreed closely with the predicted yield.
The predicted yield was 87.0 ± 4.0% which was close to the experimental yield of 86.0 ± 1.2%.
The optimum predicted yield was 57.6% whereas the experimental yield obtained was 58.0 ± 2%.
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