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The complete assignments of NMR data are displayed in Tables 2.
The complete assignments of the vibrational spectra (IR&Raman) were made with the aid of calculated spectra both in gaseous and aqueous phases.
The complete assignments of H and C NMR signals of 1 were furnished from the NOESY and HMBC spectra.
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A series of copolymeric models were synthesized to make the complete assignment of all the signals appearing in the spectrum of the tetrapolymer.
The glycolipid 1-O-palmitoyl-2-O-stearidonoyl-3-O-β-D-galactopyranosylglycerol (4) was obtained from the brown alga Sargassum incisifolium and for the first time, we report the complete assignment of its 1H NMR and 13C NMR data.
The complete assignment of spectra recorded by us in the present measurements is presented in Table 1.
This was confirmed by the complete assignment of CXCL12γ residues, but K1, E73 and K84 (Fig. 1B).
The complete assignment of the backbone amide resonances of both proteins [11], [12] allows for a residue-specific analysis of the proton exchange rates (Fig. S7, S8 and Table S1).
The complete assignment is presented in Table 1.
The complete assignment of H and C NMR spectra is listed in the Experimental Section.
Recent advances in this technology have allowed the complete assignment of resonances for several unfolded and partially folded proteins, as well as for the several IDPs and IDRs.
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