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The temperature was held at 250°C for 10 min before cooling down to 40°C.
Subsequently, the temperature was held at 4°C.
The ion source temperature was held at 250°C.
The drying temperature was held at 70°C to avoid glucose caramelization [23, 33, 34].
The temperature was held at the peak temperature for 60, 90, 120 min, respectively.
For all steps, the substrate temperature was held at 500°C.
The temperature was held at 80 °C for 24 h while being vigorously stirred.
Then, the oven temperature was held at 345 °C for 1 h.
The temperature was held at 950 °C for 30 min and then cooled to room temperature.
Thereafter, the sample temperature was held at 400 °C for 1 h.
GC conditions were the following: injector temperature was held at 240 °C, detector temperature was set at 270 °C.
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