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These factors were divinylbenzene (DVB) content, plus three factors associated with pyrolysis (peak temperature, hold time, and temperature ramp rate).
The effect of high temperature hold time at 1050 °C on thermal fatigue properties and failure characteristics of electron beam-physical vapor deposited (EB-PVD) thermal barrier coated samples (TBCs) was investigated in this work.
It is found that the concept of a damaged zone can be a successful explanatory model for the observed crack growth behavior under high temperature hold time.
In this work, two types of non-constant condition tests were run, tests in which the temperature was changed part way through the cyclic life and a second type of test where the high temperature hold time was changed part way through the cycle life.
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The interaction between three variables i.e. sintering temperature, holding time and heating rate was studied and modeled.
Effects of fabrication conditions (i.e., sintering temperature, holding time and casting temperature) on microstructure of the fabricated copper/diamond FGMs were investigated.
The result of this experiment allowed a design of heat treatment conditions for Bi-2212 block processing, including maximum processing temperature, holding time, cooling rate and annealing time.
Several experiments have been conducted according to a central rotatable design in which reaction temperature, holding time and NaOH concentration were varied and different aspects have been observed.
The best sintering results obtained for the sintering temperature, holding time, and pressure are 1700 °C, 487 s, and 49 MPa, respectively.
Parameters such as sintering temperature, holding time and sintering pressure were considered to tune the grain size, density, microhardness, bubble formation and impurity contents.
Moreover, the carbon content decreased with increasing of temperature, holding time and NH3 concentration, but contrarily, increased with enhancement of heating rate.
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