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These factors were divinylbenzene (DVB) content, plus three factors associated with pyrolysis (peak temperature, hold time, and temperature ramp rate).
While the grain size and texture are unaffected due to the high temperature hold, the volume fraction of Ʃ3 twin boundaries was found to increase significantly.
It is found that the concept of a damaged zone can be a successful explanatory model for the observed crack growth behavior under high temperature hold time.
Adding a temperature hold during rewarming at the glass transition temperature may reduce the thermo-mechanical stress in some cases, but may have an adverse effect in other cases.
The effect of high temperature hold time at 1050 °C on thermal fatigue properties and failure characteristics of electron beam-physical vapor deposited (EB-PVD) thermal barrier coated samples (TBCs) was investigated in this work.
The assessment contrasts the influence of simple and stepwise (intermediate temperature hold) thermal cycles on the undulation of the surface and on the evolution of residual compressive stress in the thermally-grown oxide (TGO) layer.
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The starting temperatures and temperature hold-times before starting fuel cell operation, the heat transfer characteristics of the hydride storage tanks, system temperature, fuel cell electrical power (including efficiency) as well as alanate kinetics were varied by system modelling with gPROMS®.
The selected process parameters were the melt temperature, mold temperature, holding pressure, holding time and cooling time.
In this study four process parameters namely, barrel temperature, mould temperature, holding pressure and injection speed were considered.
To apply a heat pulse, the furnace temperature was increased by 10 °C from the growth temperature, held for 2 min and then cooled to the initial growth temperature.
The interaction between three variables i.e. sintering temperature, holding time and heating rate was studied and modeled.
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