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(a) Synthetic procedure of the Spacer molecules.
(b) Synthetic procedure of the drug-conjugated and surface-modified AuNPs.
The research examined a novel one-step synthetic procedure of bioactive 3-arylazo-substituted coumarin derivatives (4i 4v) and further evaluated their biological actions.
The synthetic procedure of hydroxyapatite was investigated in detail to determine the influence of numerous parameters such as pH of reaction mixture, ATRP initiator concentration, dilution of ammonium hydroxide, on the final properties of the particles.
Fig. 1 Synthetic procedure of GNR-SiO2-Ab.
Graphical abstract The improved synthetic procedure of lesinurad (I).
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In the frame of research aimed at developing new synthetic procedures of multimetallic Nb-based catalysts, peroxo complexes of niobium V) of general formula AI3[Nb(O2)4] and AI3[Nb(O2)x HyL)]·nH2O (AI: NH4+, CN3H6+ (gu); L: oxalate, tartrate, citrate) have been prepared and characterized on the basis of elemental and thermal analysis, FTIR and 13C-NMR spectra.
In this paper, inspired by the cubic bi-continuous gyroid structure self-assembled by block copolymers, we start with the application of a novel and more facile approach, compared to the tedious synthetic procedures of block copolymers, to prepare the bi-continuous phases structured nanocomposite electrolytes.
Scheme 1 Synthetic procedures of methyl matrinate and matrinol derivatives.
Figure 1 shows the synthetic procedures of conventional preparation with (a) a sulfo-SMCC cross-linker from amino-silaneMNPs@SiO2 and (b) a one-step preparation with a chloro-silane functional group on MNPs@SiO2.
In comparison to DGO-OH [21], the relative intensity of the C-C peak remains the same after esterification, but the intensity of the C = O and O-C = O peaks increased, which may be due to increased functionality. Figure 1 Schematic representation of the synthetic procedures of the graphene-polymer nanocomposites.
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