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The F1 dimension covered 3.2 kHz sweep width with 256 increments.
The F1 (13C) dimension covered 33 kHz sweep width with 128 increments.
Usual parameters included 42-ms acquisition time with sweep width of 30 kHz; 2 K data points were collected.
The samples were measured at 90 K with center field 3500 G and sweep width 5000 G.
1H NMR spectra was recorded at the same concentration of lignin without using a sweep width of 9600 Hz.
DEPT spectra were recorded with 12,000 acquisitions, 10 s recycle delay, and 42 kHz sweep width.
For continuous-wave electron paramagnetic resonance spectroscopy, what settings of magnetic field sweep width and field modulation amplitude yield the best accuracy in estimated linewidth?
The sweep width of the 2D homonuclear TOCSY and ROESY spectra was 5592.84 Hz in the direct and indirect 1H-dimension, respectively.
Carbon spectra were acquired with a sweep width of 34,722 Hz using an acquisition time of 0.4 s and a relaxation delay of 1.6 s.
[21 23]13C spectra were recorded with 22,000 acquisitions, 10 s recycle delay, 9 μs pulse width (70°) and 33 kHz sweep width.
1H spectra were recorded with 1000 acquisitions, 4 s recycle delay, 4 μs pulse width (70°) and 6 kHz sweep width.
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