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It was evident that the hydration products and internal structures of the specimens were unaffected by the repetitive heating and the ionically-conductive mortar maintained stable electrical conductivity.
The crystalline structures of the specimens were analyzed by X-ray diffraction (XRD) patterns.
The capillary water absorption results representing the changes in pore structures of the specimens are presented on the left side of Fig. 6.
Full-profile Rietveld refinement of Nd1-x Sr x Al1-x Ti x O3 structures, performed in space groups R ( overline{3} ) c and Pm ( overline{3} ) m for the samples with x ≤ 0.8 and x = 0.9, respectively, entirely confirms suggested crystal structures of the specimens.
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Our study shows that the dielectric properties are strongly dependent on the compositions, densification and micro-structure of the specimens.
In addition, the changes in the internal micro-structure of the specimens resulted from variations in the stress condition, were found to affect the ultrasonic velocity measurements.
In addition, SiO2 nanoparticles are able to act as nanofillers and recover the pore structure of the specimens by decreasing harmful pores.
In addition, the internal structure of the specimens was analyzed using a scanning electron microscope (SEM) and by micro-computed tomography (Micro-CT) analyses.
An X-ray computed tomography (X-ray CT) system was used to capture the internal structure of the specimens and image analysis techniques were used to quantify the distribution of air voids.
The internal structure of the specimens was observed by using a transmission electron microscope (TEM).
The deviation from a precise round form is mainly the discrete atomic structure of the specimens.
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