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The stirring was maintained during the electrodeposition.
Strong magnetic stirring was maintained for 3 h.
The stirring was maintained for 15 min, and SiO2 films with a thickness of ~20 nm were formed.
The stirring was maintained for 4 hours at 40°C in order to ensure the maturation of the PU structures walls, even if the structures were formed in the first three minutes.
Soon after adding H2TPyP chloroform solution, an opaque solution was obtained; a transparent yellowish solution was obtained after vigorous stirring was maintained for 15 min, as shown in Figure 1.
Subsequently, in order to facilitate the collection of the particles, 25 mL of Milli-Q water was added to the nanoparticles suspension, and the stirring was maintained for 10 min. Finally, the organic solvents were eliminated by evaporation under vacuum at 37 °C and the blank nanoparticles were collected.
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(D) Solution obtained after stirring is maintained for 15 min. On the basis of the aforementioned brief review, we herein investigate the assembly behavior of H2TPyP via a process similar to that for ZnTPyP [39].
The stirring was maintaining for 10 min before the formulation was fed into the spray dryer.
In a typical experiment [ 14], 0.01 mol/L of chloroauric acid (5 mL) and 1% sodium citrate (10 mL) were added to 50 mL of an aqueous solution that had been heated and stirred until reaching the boiling point; heating and vigorous stirring were maintained until the solution reached a wine red color.
As coagulant was added, stirring speed was maintained at 100 rpm for 2 min and followed by a slow stirring speed of 40 rpm for 10 min, (Choy 2016).
Therefore, the solution stirring speed was maintained at 500 rpm to isolate the gas-injection flow rate and Au concentration effect on nanoparticle synthesis.
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