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Volatiles of the filtrate were removed under reduced pressure to afford a sticky solid (1.00 g).
Volatiles of the greenish filtrate was removed under reduced pressure to afford a sticky solid (0.390 g) that was purified by column chromatography (Si gel, 100 to 200 mesh) using 30% methanol-ethyl acetate as the eluant affording a greenish solid (0.3 g).
Knead the ingredients together until a sticky, solid clay forms.
The resulting aqueous solution was lyophilized to give AHP2TFA as a white sticky solid (0.034 g, 25%).
The resulting aqueous solution was lyophilized to give 10b2TFA as a white sticky solid (0.032 g, 22%).
Poly vinyl acetate) was then recovered as a yellow sticky solid after precipitation into hexane.
Similar(54)
In these cases, proteins aggregate and spontaneously transition from a liquid phase into a sticky, solid-like state, prohibiting normal function in the brain or nervous system.
The application of the jet spouted bed as a reactor in catalytic polymerizations implies the treatment of sticky solids with a wide particle size distribution, even of catalyst particles of reduced size (less than 1 mm diameter), which are not habitually treated in conventional spouted beds.
Sodium bisulphite (9.3 g, 89.4 mmol) in water (30 ml) was added then the mixture was refluxed for 3 h, cooled and poured into water to give sticky solids.
The light brown solution was dried by rotary evaporation to yield a sticky brown solid.
The water fraction was sticky and solid while that of n-butanol and chloroform fractions were jelly.
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