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Then, 0.5 mL of starch indicator solution was added.
About 10 drops of starch indicator was added to the sample.
The mixture is titrated with 0.01 mol/L sodium thiosulfate standard solution to the color of buff; successively by added starch indicator, continuing titrated with the sodium thiosulfate standard solution to the color of blue disappearing as the titration end point [19].
The starch indicator solution and the iodine reagent were prepared.
* starch indicator solution: mix 5 g starch with a little cold water and grind in a mortar.
Iodometric titration with 0.1 M Na2S2O3 solution and a starch indicator was performed after acidification with 2 N H2SO4.
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Hypochlorite residues can be detected by putting some decapsulated cysts in a small amount of starch-iodine indicator (= starch, KI, H2SO4 and water).
Dissolved oxygen concentrations were determined by automated high-precision Winkler titration with a potentiometric end-point Metrohm 808 Tinrando28 in the Svalbard communities and using starch as indicator for end-point detection in the Young Sound communities.
Next, 2 mL of idodine-oxalate titrated with 0.005 N sodium thiosulfate was added using starch as indicator.
For the quantitative determination of iodine, one of the following methods may be recommended: (1) gravimetrically, by precipitation as silver iodide; (2) volumetrically, by titrating iodine with a standardized solution of sodium thiosulfate (using starch as an indicator); or (3) potentiometric titration with silver nitrate, which is applicable in the presence of both chloride and bromide.
The reduced copper was quantified by idometric titration using starch as an indicator.
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