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All tests were performed in the fasting state between 08.00 and 14.00 h. at standard room temperature.
All rats were housed in cages one week before the experiments in an acclimatized room at standard room temperature and with twelve hour light/dark cycles.
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The first trialkoxysilane was N- triethoxysilylpropyl -O-polyethylene oxide urethaN- triethoxysilylpropyl -O-polyethyleneol, aN- triethoxysilylpropyl -O-polyethyleneeoxy)propyl]-trimethoxysilaN- triethoxysilylpropyl -O-polyethyleneoxidend they were urethaneend link hydroxyl-terminated PDMS1chains in standard room-temperature condensation reactions.
Relaxation dispersion (CPMG) experiments were performed at 50 °C using an ∼1.5 mM U-[N,H], ILV CH3 sample on 500 and 800 MHz Varian Inova spectrometers equipped with standard room-temperature triple-resonance probes.
The DNP-enhanced C-labeled substrates, once dissolved in hot water, have to be rapidly transferred into the bore of the MR system to minimize the C polarization losses occurring through longitudinal spin relaxation processes (the standard room-temperature T1 of C-labeled metabolic substrates is shorter than 1 min).
NMR spectra were obtained on Bruker Avance 800 MHz and Bruker Avance III 500 spectrometers with tetramethylsilane as an internal standard at room temperature.
The mechanical strength as well as the electrical conductivity depend on the grain size of the Cu matrix, which can be influenced by the temperature of the heat treatment, i.e., a mechanical strength of about 1.6 GPa is measured for a Cu 10 at.% Nb alloy which shows an electrical conductivity of about 10% IACS (international annealing copper standard) at room temperature.
NMR spectra were acquired on Bruker AM-400, DRX-500 and Avance III 600 MHz spectrometers with tetramethylsilane (TMS) used as an internal standard at room temperature.
NMR spectra were acquired with instrument of a Bruker DRX-600 with tetramethylsilane (TMS) used as an internal standard at room temperature.
Diffuse reflectance spectra were recorded with respect to the BaSO4 standard at room temperature by means of double-beam spectrophotometer UV-3600 UV-VIS NIR (Shimadzu Company) equipped with an integrated sphere ISR-3100.
IPS/MnTSPP has proved able to efficiently degrade all tested dyes, regardless of their chemical class, under very mild conditions: standard pressure, room temperature and neutral pH, using no organic solvents, and the most environmental-friendly oxidant.
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