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The transformation process from ZIF-67 to Co3O4 hollow sphere was characterized by powder X-ray powder diffraction, scanning electron microscopy, transmission electron microscopy, Fourier transform infrared spectroscopy, and thermal gravimetric analysis.
The crystalline structure of the as-synthesized ZnFe2O4 hollow sphere was characterized by powder XRD.
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In the BCE process, the early stage of CaSO4 precipitated onto the surface of nano-sized silica spheres was characterized using dynamic light scattering, zeta potential analysis and atomic force microscopy imaging, which indicated that a coating was produced on the silica surface.
Spatial arrangement of the silica spheres was characterized by scanning electron microscope (SEM; Zeiss EVO 50, Oberkochen, Germany).
The photoelectrochemistry of electrodes based on nitrogen-doped and undoped TiO2 spheres was characterized with Mott-Schottky analysis, intensity modulated photocurrent spectroscopy, and electrochemical impedance spectroscopy, which indicated that both the quasi-Fermi level and the charge transport of the photoelectrode were improved after being doped with nitrogen.
The formation of covalent bonds between solid surface-nanosphere and sphere-sphere was characterized using FTIR spectroscopy.
Supercapacitor electrodes based on the NiO hollow spheres are characterized.
The functionalized glassy carbon spheres were characterized electrochemically by studying their cyclic voltammetry.
The as-prepared silica spheres were characterized by elemental analysis, scanning electron microscopy, mercury porosimetry and nitrogen sorption measurements.
The obtained TiO2 hollow spheres were characterized by X-ray diffraction, scanning electron microscopy, transmission electron microscopy, N2 adsorption desorption analysis, and UV visible diffuse reflectance spectroscopy.
Prepared active carbon spheres were characterized using scanning electron microscope, surface area analyzer, thermo gravimetric analyzer, tensile tester, and CHNS instrument.
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