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An organic inorganic hybrid paratungstate [enH2]2[Cu en 2]3[H2W12O42]·6H2O (1) (en = ethylenediamine) has been hydrothermally synthesized by reaction of Na2WO4·2H2O with CuCl2·2H2O in the presence of en and structurally characterized by elemental analyses, IR spectroscopy, UV spectrum, powder X-ray diffraction (PXRD), thermogravimetric analysis (TGA) and X-ray single-crystal diffraction.
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The synthesized Ag colloids have been characterized by UV-visible spectra, powder XRD, HRTEM, and selected area electron diffraction (SAED).
The primary CL mechanism is proposed based on CL spectra, powder X-ray diffraction (XRD), high-resolution transmission electron microscopes (HRTEM) and fluorescent spectra, etc.
These complexes were characterized by elemental analysis, IR spectra, powder X-ray diffraction (PXRD), thermogravimetric (TG) analysis and single-crystal X-ray diffraction.
In addition, elemental analysis, IR and UV Vis spectra, powder X-ray diffraction patterns, thermogravimetric analyses of these complexes have been investigated.
In addition, the high quality of the resulting CdS NCs was confirmed by the PL spectra, powder X-ray diffraction (XRD), and high-resolution transmission electron microscopy (HRTEM).
Their structures have been determined by single-crystal X-ray diffraction analysis and further characterized by elemental analysis, IR spectra, powder X-ray diffraction (PXRD), and thermogravimetric (TG) analysis.
A novel metal organic complex [Fe(H2bpdc)]SO4 (1) has been hydrothermally synthesized (H2bpdc = 2,2'-bipyridyl-5,5'-dicarboxylic 2,2'-bipyridyl-5,5'-dicarboxylic 2,2'-bipyridyl-5,5'-dicarboxylic 2,2'-bipyridyl-5,5'-dicarboxylicnd single-crystacid-randdiffraction, which distructurallyirst 1-D ferrous sulfate characterizednalized by H2bpdc.
Before measuring FTIR spectra, powders were triturated in the agate mortar.
The compounds were characterized by Infrared spectrum and powder x-ray diffraction patterns.
Fig. 5 FTIR spectrum of powder prepared by laser ablation of Mg in acetone.
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