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Figure 7 Raman spectrum of sample L5.

(a) R specular spectrum of sample R-OSC(1).

The spectrum of sample 1 is magnified tenfold.

Figure 8c shows the Raman spectrum of sample zb2-3.

Fig. 5 a XRD spectrum of N26 sample; b XRD spectrum of sample N21; c comparative XRD spectrum of sample N23 before and after the treatment; d comparative XRD spectrum of sample N25 before and after the treatment.

FT-IR spectrum of sample 1 as an example is depicted in Fig. 1.

The percentage of Na+ in the EDX spectrum of sample NZ is low.

Fig. 6 Raman spectrum of sample YLS2-2 (pyromorphite, cerussite and cuprite)  .

The FTIR transmission spectrum of sample A presents typical characteristics of the IR properties of ZnO.

Figure 2 EDS spectrum of sample A and EDS mapping for Au and Ag elements.

Figure 6 Raman spectrum of sample P3 (A) and L2 (B).