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Surface modification of carbon nanotubes by PEI can be observed through TEM, SEM, and FTIR spectroscopy (Figures 2, 3, and 4) as well as the dramatic change in zeta potentials (Figure 7), and the amount of grafted PEI was estimated by TGA (Figure 5).
We noticed on day 21 (across all treatments) that exudate yields had declined (Figure 2) relative to earlier collections on days 7 and 14. 1H NMR spectroscopy (Figures 3,4,5) demonstrated differences in exudate profiles under the influence of the treatments, and PCA analysis revealed significant changes from day 14 onward (Figure 6).
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The composition of the particles was confirmed by FTIR spectroscopy (Figure S2).
Complementary information can be obtained from Raman spectroscopy (Figure 5).
Complementary information can be obtained from FT-Raman spectroscopy (Figure 7).
The higher dye loading capability of the HNF is validated using UV vis spectroscopy (Figure 4b).
The reaction was monitored in real time by using UV-vis spectroscopy (Figure 4).
These NFs were further characterized using Fourier transform infrared (FTIR) spectroscopy (Figure 3).
The successful synthesis of graphene and Au nanoparticles decorated graphene was confirmed by ultraviolet-visible (UV-Vis) spectroscopy (Figure 1).
Elemental composition analysis by energy dispersive X-ray spectroscopy (Figure 4) also proved RC binding to PSiMc.
Information about the chemical structure of the components of the various extracts was obtained using FT-IR spectroscopy (Figure 1).
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