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Topography of bare specimen, blank, specimens treated with 0.5 mM CPFASC and NPFASC in 1 M HCl for 24 h are given in Fig. 13a d, respectively.
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This paper describes the results of analytical work undertaken to investigate factors that can influence the magnitude and distribution of residual stresses retained in fracture mechanics specimen blanks extracted from as-welded ferritic and austenitic stainless steel plates.
The results indicate that significant levels of residual stress can be retained in specimen blanks prior to notching, and that the magnitude and distribution of stress is dependent upon material properties, specimen geometry and size, and extraction location through the thickness of the weld.
The approach can help guide the selection of specimen geometry and machining strategies to minimise the level of residual stresses retained in fracture mechanics specimen blanks extracted from non stress-relieved welds and thus improve the measurement of weld fracture toughness properties.
Then 100 µl of a 10-fold dilution of the serum specimen, a blank, a positive and a negative reference serum sample were each added to a separate well.
The fracture mechanics specimens were blank hardened in order to have the core properties of the notched specimens.
Limits of detection were calculated as three times the standard deviation of near-zero or blank quality control specimens.
A Pockels cell modulator (model 350-80LABK, Conoptics, Danbury CT) synchronized to the laser scanner was used to blank the laser beam during fly-back so that the specimen was illuminated only while pixel data was being collected.
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