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The crude extract was suspended in 5 mL 50% MeOH H2O and was passed through a C-18 SPE (1 g) column.
The SPE cartridges were first activated with ethyl acetate, followed by methanol and equilibration with water (for SPE, 1 mL and for μelution SPE, 200 μL of each were used).
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Briefly, Supelclean LC-18 SPE cartridges (1 mL, 100 mg; Sigma-Aldrich, St . Louis MO, U.S.A).
In order to improve the parameters of process, increase the yield and reduce the corrosion during the synthesis of the Phosphonate-PEG polymers for SPE, 1-methylimidazole as an acid scavenger was used.
SPE 105327, 15th SPE Middle East Oil & Gas Show and Conf., Bahrain, Mar.
Paper SPE 29488 presented at the SPE Production Operations Symposium, Oklahoma City, Oklahoma, 2 4 April.
We use the one-step deviation principle to prove this SPE [10, 19].
For comparison, the QYs from OIP polycrystalline thin films were <10% for spontaneous emission (SPE) and ∼15% for amplified SPE [125].
Liquid-liquid extraction (LLE) [16, 19, 21] and solid phase extraction (SPE) [20, 21, 26] are often used to determine the EC content in alcoholic beverages.
The presented procedures included acid (hair) or enzymatic (urine and meat) hydrolysis, C18 reversed-phase SPE, Na2CO3 liquid liquid clean-up and SiOH normal-phase SPE.
Using the threshold value for MC detection of Zr=1.86, the PPPM showed greater sensitivity (94.6%) in detecting a MC compared to either SPE (64.8%) or KLR (89.2%).
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