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The solution was heated for 5 min.
and the solution was heated to boiling point.
The solution was heated to 150 °C for 5 h.
The aqueous solution was heated for 12 h under reflux.
Then the solution was heated to 290 °C.
The solution was heated and stirred for an hour.
Further, the solution was heated to 100 °C.
The solution was heated at boiling point under continuous stirring.
The solution was heated for 1 h at 50°C.
The solution was heated at 65 °C for 2 h.
The solution was heated to 50 °C for 20 min.
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