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A solution of compounds 22a b (0.01 mol) in acetic anhydride (10 mL) was heated for 15 min.
A solution of compounds in a mixture of acetic anhydride pyridine (1 1) were stirred fully and settled at 25 °C for 12 h.
To boiling solution of compounds 10a b (0.01 mol) in ethanolic potassium hydroxide (30 mL, 10%), thiourea (0.01 mol) was added.
The CH2Cl2 solution of compounds 5 and 6 obeyed the Beer Lambert law in the concentration range of 10−8 10−3 M.
Compound 2 showed a strong association tendency in CH2Cl2 but no aggregates could be detected in the solution of compounds 4 6.
This experimental evidence for the conformations in solution of compounds 2 5 was provided by rotating frame Overhauser effect spectroscopy (ROESY) experiments conducted in DMSO; the significant NOE signals are indicated in Fig. 3.
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PhIO (0.11 mmol) was added to a solution of compound 1 (0.1 mmol) in MeOH (2.0 mL) at 25 °C.
The method is particularly suitable for the solution of compound contact problems such as for example the fitting calculations of shafts with rolling bearings.
To a solution of compound 4 (1.10 g, 6.75 mmol) in ethanol (12 mL), Conc.
The single crystal was obtained by slow evaporation of a solution of compound 10g in ethyl acetate at room temperature.
A solution of compound 3 (50 mmol) in THF (100 mL) was then added to the reaction mixture at this temperature.
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