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The above solution is evaporated and crystallized to obtain rare-earth chlorides (LnCl3).
The solution is evaporated in a drying oven at 110 °C, the residue is dissolved in 0.5 ml of MeOH/THF (1 1), and then filtered.
The vial is kept at 70°C for 20 min; it is then removed from the heat, left to stand until cool, and the solution is evaporated using a nitrogen stream to syrup or dryness.
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The solution was evaporated in a rotary evaporator flask under vacuum at the bath temperature of 70 °C to 30 ml.
In a typical digestive ripening, a batch of as-prepared Au NPs solution was evaporated for about 35 °C by rotary evaporation to get rid of the solvent.
The trap solution was evaporated to dryness using a rotary evaporator (Buchi, V-850, Switzerland) at 40 °C, then re-suspended in 100%% methanol and re-evaporated twice.
40 μL of this solution was evaporated to dryness in a centrifugal evaporator and was then dissolved in 10 µL of 50%% (v/v) acetonitrile.
The filtered n-hexane solution was evaporated at 40°C using a rotary evaporator until a volume of 1 mL was obtained.
The resultant solution was evaporated under vacuum in a rotary evaporator to obtain a dry mass extract (yield: 14.36% w/w).
Lastly, the solution was evaporated in a petri dish to reduce the duration of complete evaporation and prevent the agglomeration of the GNPs.
The solution was evaporated to dryness.
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