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After 7 days, solids were collected from all four treatments.
Control reactors with an identical buffer system, Mn solids loading, and Fe/Mn ratio were mixed for 90 min before solids were collected and resuspended in deionized water.
At the end of the experiment, the solids were collected by centrifugation (10,000 rpm/min) and filtration and then were washed thoroughly by using ethanol and deionized water.
At the end of the dissolution experiment, the solids were collected from the bottles, rinsed, dried and characterized using XRD, FT-IR, FE-SEM and FE-TEM instruments in the same manner as previously described.
The reaction mixture was heated to reflux for five hours, cooled and the precipitated solids were collected by filtration to give the ketones 3a-d which were pure enough to be used in the next step.
Solids were collected into acid-washed jars, and major and trace elements determined by ICP-AES/ICP-MS on aqua regia extracts of air-dried material (Chemex Labs, Sparks, NV).
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Sand solids are collected and monitored throughout the experiment, which lasted approximately 1300 min.
The resulting solid was collected and crystallized from ethanol to give (20a d), respectively.
The resulted solid was collected by magnetic field and washed with ethanol and dried at 60 °C.
After cooling, ethanol was added and the precipitated solid was collected by filtration.
Stoichiometric data for the CSH solid was collected from a t = 21 h reacted sample.
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