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Conductivity and pH were measured at 25 °C respectively without disturbing the settled solids using an EC Testr 11 Dual range 68X 546 501 m (Eutech Instruments, Singapore) and a Hanna HI8 424 pH meter (Hanna Instruments, Woonsocket, RI).
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It is possible that this could be due to the presence of an undetected second phase since Rozov et al. determined the composition of their solids using a bulk technique.
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