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The solids collected from the three replicates for a given treatment and time period (e.g. T1, 24 hours) were combined to attain sufficient mass for analysis.
SEM examination of the AC solids collected after 1 day showed agglomerations of roughly spherical particles on the order of 100 nm in diameter (Figure 3a).
Complexity and variety in centrifuge design is largely due to a need to dispose of solids collected in the separation zone.
Rietveld structure refinement was performed on diffraction patterns obtained from solids collected at the end of the experiment (7 days) to confirm phases, refine lattice parameters and estimate crystallite dimensions.
Figure 3 Representative SEM images of solids collected from the four treatments during the course of the experiment: (a) treatment AC after 24 hours, (b) treatment HC after 72 hours, (c) treatment AC after 7 days, (d) treatment OA after 7 days, (e) treatment LC after 7 days, and (f) treatment HC after 7 days.
The tube was allowed to cool and the solids collected by filtration.
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Instead of a flush, the toilet uses a scraper mechanism that sends the waste from the toilet bowl into a collection tank below, where the solids collect at the bottom as sediment and where the liquid waste is filtered.
In contrast, the solid collected by destabilization of the colloid solutions is composed of agglomerated nanoparticles (Figure 3). Figure 3a,b shows field emission gun-SEM images of the as-obtained solid.
The concentrated filtrate was sonicated in hexanes (20 mL/mmol) and the solid collected by filtration to give the product, which was purified by recrystallization from acetone.
The white solid collected by freeze-drying was further extracted with cold methanol for 24 h to remove rests of the PNIPAAM homopolymer.
The washed solids were collected to determine moisture content and calculate the solid recovery from IL pretreatment.
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CEO of Professional Science Editing for Scientists @ prosciediting.com